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Mineralogy & Geochemistry Laboratories Structural analysis Malvern-Panalytical EMPYREAN

Empyrean Empyrean diffractometer (Malvern-Panalytical): Ambient and Non-Ambient PXRD - HTK 1200 

The ‍Malvern ‍- ‍Panalytical ‍EMPYREAN ‍X-ray diffractometer ‍is ‍with ‍einer ‍Mo ‍or ‍ Cu ‍- ‍LLF ‍- ‍tube, ‍einer ‍AntonPaar ‍HTK ‍1200N ‍Hochtemperatur ‍- ‍Ofenkammer ‍und ‍einem ‍hochmodernen ‍Röntgendetektionssystem, ‍dem GaliPIX3D ‍(with ‍fast ‍100 ‍% ‍Wirkungsgrad ‍für ‍hochenergetische ‍Mo radiation) ‍ausgestattet. ‍This ‍arrangement ‍enables ‍qualitative ‍high-quality ‍& ‍high-resolution ‍data acquisition ‍for ‍space- ‍und high-temperature experiments ‍( ‍bis ‍1200 ‍°C ‍in ‍der ‍Luft ‍) ‍in ‍Reflexions- ‍oder ‍Transmissionsgeometrie

Empyrean Diffraktometer (Malvern-Panalytical) © AG MinGeO

Empyrean Diffraktometer (Malvern-Panalytical) © AG MinGeO

  • ‍ ‍‍Grid parameter refinement
  • ‍ ‍‍Heat expansion coefficients
  • ‍ ‍‍Structure determination
  • ‍ ‍‍‍Investigation ‍of ‍phase relationships
  • ‍ ‍‍Studies ‍on ‍chemical ‍reactions
  • ‍ ‍‍‍Dynamic ‍structural changes
  • ‍ ‍‍Capillaries:
    • ‍Measurement ‍of ‍air-sensitive ‍samples ‍and/or ‍small ‍sample volumes,
    • ‍reduction of preferential ‍orientation effects

Empyrean diffractometer - Tomography Malvern-Panalytical EMPYREAN: PXRD tomography 

The ‍Malvern-Panalytical ‍EMPYREAN ‍X-ray diffractometer ‍ist ‍with ‍a ‍Mo-LFF tube ‍(or ‍Cu tube), ‍einem ‍Rotary sample well ‍für ‍CT ‍und ‍einem ‍hochmodernen ‍Detektionssystem, ‍dem ‍GaliPIX3D, ‍ausgestattet, ‍das ‍in ‍der ‍Lage ‍ist, ‍Daten ‍zu ‍sammeln, ‍die ‍für ‍die ‍3D processing ‍in ‍der ‍Computertomographie ‍geeignet ‍sind.‍Computed tomography ‍(CT) ‍provides ‍the ‍possibility to analyse ‍various ‍properties ‍(e.g. ‍quantity/type/connectivity ‍of ‍pores, ‍Rissen, ‍Einschlüssen, ‍Mineralverteilung, ‍Vorzugsrichtungen, ‍Wanddicke, ‍Oberfläche) ‍durch ‍dreidimensionale ‍virtuelle ‍Rekonstruktionen ‍der ‍Probe ‍schnell ‍und ‍zerstörungsfrei ‍zu ‍analysieren ‍und ‍zu ‍visualisieren.

Empyrean - Tomographiemodul © AG MinGeo

Empyrean - Tomographiemodul © AG MinGeo

  • ‍Building materials‍
  • ‍Ceramics‍
  • ‍Composite materials‍
  • ‍Foams
  • ‍Electronics
  • ‍Stones

  • Mo- ‍or ‍Cu- ‍LFF tube ‍at ‍point focus
  • Incident ‍beam optics ‍& filter
  • CT ‍Rotational probe
  • ‍Sample holder ‍with ‍Sample
  • GaliPIX3D ‍detector
  • Experimental ‍parameters ‍(anode material, ‍voltage/current, ‍filter materials, ‍rotation range, ‍step size, ‍time ‍per ‍step, ‍PHD values) ‍können ‍entsprechend ‍der ‍Probe ‍eingestellt ‍werden.

Tomography - application example Example: ‍Autocalised ‍porous concrete 

‍The ‍3D pore size distribution ‍(which ‍has ‍an ‍influence ‍on ‍strength, ‍permeability, ‍density, ‍thermal insulation ‍usw. ‍has) ‍can ‍be determined with ‍CT ‍on ‍an ‍X-ray diffractometer ‍in ‍the ‍laboratory ‍ ‍und ‍visualisiert ‍werden.

Autokalivierter ‍Porenbeton

Autokalivierter ‍Porenbeton.- Tomographieaufnahme

Laboratories

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